Racemic 9,10-dimethoxy-3-methyl-6-phenyl-7,7a-dihydrobenzo[b]benzo[4,5]isothiazolo[2,3-d][1,4]diazepine 12,12-dioxide

J.P. Bassin; V.P. Shah; L. Martin; P.N. Horton

doi:10.1107/S1600536811004983

Racemic 9,10-dimethoxy-3-methyl-6-phenyl-7,7a-dihydrobenzo[b]benzo[4,5]isothiazolo[2,3-d][1,4]diazepine 12,12-dioxide

J.P. Bassin
, V.P. Shah
, L. Martin
, P.N. Horton

Research output: Contribution to journal › Article › peer-review

2 Citations (Scopus)

97 Downloads (Pure)

Abstract

There are two molecules in the asymmetric unit of the title compound, C24H22N2O4S. The conformation of the seven-membered ring is twisted boat for both molecules. The molecule is chiral, but crystal symmetry generates a recemate. The crystal packing is stabilized by weak intermolecular C-HO hydrogen bonds.

Original language	English
Journal	Acta Crystallographica Section e
Volume	67
Issue number	3
DOIs	https://doi.org/10.1107/S1600536811004983
Publication status	Published - 2011

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@article{3d364dfcafde4ae29ca228e8065710b6,

title = "Racemic 9,10-dimethoxy-3-methyl-6-phenyl-7,7a-dihydrobenzo[b]benzo[4,5]isothiazolo[2,3-d][1,4]diazepine 12,12-dioxide",

abstract = "There are two molecules in the asymmetric unit of the title compound, C24H22N2O4S. The conformation of the seven-membered ring is twisted boat for both molecules. The molecule is chiral, but crystal symmetry generates a recemate. The crystal packing is stabilized by weak intermolecular C-HO hydrogen bonds.",

author = "J.P. Bassin and V.P. Shah and L. Martin and P.N. Horton",

note = "Original article can be found at: http://scripts.iucr.org/ Copyright International Union of Crystallography This open-access article is distributed under the terms of the Creative Commons Attribution Licence http://creativecommons.org/licenses/by/2.0/uk/legalcode, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.",

year = "2011",

doi = "10.1107/S1600536811004983",

language = "English",

volume = "67",

journal = "Acta Crystallographica Section e",

issn = "1600-5368",

publisher = "International Union of Crystallography",

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TY - JOUR

T1 - Racemic 9,10-dimethoxy-3-methyl-6-phenyl-7,7a-dihydrobenzo[b]benzo[4,5]isothiazolo[2,3-d][1,4]diazepine 12,12-dioxide

AU - Bassin, J.P.

AU - Shah, V.P.

AU - Martin, L.

AU - Horton, P.N.

N1 - Original article can be found at: http://scripts.iucr.org/ Copyright International Union of Crystallography This open-access article is distributed under the terms of the Creative Commons Attribution Licence http://creativecommons.org/licenses/by/2.0/uk/legalcode, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.

PY - 2011

Y1 - 2011

N2 - There are two molecules in the asymmetric unit of the title compound, C24H22N2O4S. The conformation of the seven-membered ring is twisted boat for both molecules. The molecule is chiral, but crystal symmetry generates a recemate. The crystal packing is stabilized by weak intermolecular C-HO hydrogen bonds.

AB - There are two molecules in the asymmetric unit of the title compound, C24H22N2O4S. The conformation of the seven-membered ring is twisted boat for both molecules. The molecule is chiral, but crystal symmetry generates a recemate. The crystal packing is stabilized by weak intermolecular C-HO hydrogen bonds.

U2 - 10.1107/S1600536811004983

DO - 10.1107/S1600536811004983

M3 - Article

SN - 1600-5368

VL - 67

JO - Acta Crystallographica Section e

JF - Acta Crystallographica Section e

IS - 3

ER -

Racemic 9,10-dimethoxy-3-methyl-6-phenyl-7,7a-dihydrobenzo[b]benzo[4,5]isothiazolo[2,3-d][1,4]diazepine 12,12-dioxide

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